{"id":29443,"date":"2024-10-17T03:16:14","date_gmt":"2024-10-17T03:16:14","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/astm-d5317\/"},"modified":"2024-10-24T14:11:14","modified_gmt":"2024-10-24T14:11:14","slug":"astm-d5317","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/astm\/astm-d5317\/","title":{"rendered":"ASTM-D5317"},"content":{"rendered":"

ASTM D5317-98-Reapproved2011<\/h3>\n

Historical Standard: Standard Test Method for Determination of Chlorinated Organic Acid Compounds in Water by Gas Chromatography with an Electron Capture Detector<\/h4>\n
\n

ASTM D5317<\/h4>\n

Scope<\/strong><\/p>\n

1.1 This test method covers a gas chromatographic procedure for the quantitative determination of selected chlorinated acids and other acidic herbicides in water. Similar chemicals may also be determined by this test method, but it is the user’s responsibility to verify the applicability of this test method to any compounds not listed in this scope. The acid form of the following compounds were interlaboratory tested using this test method, and the results were found acceptable:<\/p>\n

Keywords<\/strong><\/p>\n

electron capture; gas chromatography; herbicides; organic acid; Chlorinated phenoxy acid herbicide; Electron-capture detectors (ECD); Gas chromatography (GC)–water; Herbicides; Organic acid; Total free acid<\/p>\n

ICS Code<\/strong><\/p>\n

ICS Number Code 71.080.40 (Organic acids)<\/p>\n

DOI:<\/strong> 10.1520\/D5317-98R11<\/p>\n<\/div>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
1<\/td>\nScope
Referenced Documents <\/td>\n<\/tr>\n
2<\/td>\nTerminology
Summary of Test Method
Significance and Use
Interferences <\/td>\n<\/tr>\n
3<\/td>\nApparatus and Equipment
FIG. 1
TABLE 1 <\/td>\n<\/tr>\n
4<\/td>\nReagents and Materials <\/td>\n<\/tr>\n
5<\/td>\nHazards
Sample Collection, Preservation, and Storage
Calibration <\/td>\n<\/tr>\n
6<\/td>\nProcedure <\/td>\n<\/tr>\n
8<\/td>\nEsterification
Magnesium Silicate Separation
Extract Storage
Chromatography
FIG. 2 <\/td>\n<\/tr>\n
9<\/td>\nCalculation
Precision and Bias <\/td>\n<\/tr>\n
10<\/td>\nTABLE 2 <\/td>\n<\/tr>\n
11<\/td>\nQuality Control
TABLE 3 <\/td>\n<\/tr>\n
12<\/td>\nTABLE 4
TABLE 5 <\/td>\n<\/tr>\n
14<\/td>\nKeywords
X1. Example Calculation Of Acceptance Criteria for Initial Demonstration Of Proficiency
X1.1 Maximum Acceptable Standard Deviation (Sm)
X1.2 Acceptance Range for Mean Recovery <\/td>\n<\/tr>\n
15<\/td>\nREFERENCES <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

D5317-98(2011) Standard Test Method for Determination of Chlorinated Organic Acid Compounds in Water by Gas Chromatography with an Electron Capture Detector<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
ASTM<\/b><\/a><\/td>\n2011<\/td>\n15<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":29444,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[1017,2637],"product_tag":[],"class_list":{"0":"post-29443","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-71-080-40","7":"product_cat-astm","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/29443","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/29444"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=29443"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=29443"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=29443"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}