BS ISO 6721-5:2019
$102.76
Plastics. Determination of dynamic mechanical properties – Flexural vibration. Non-resonance method
| Published By | Publication Date | Number of Pages |
| BSI | 2019 | 18 |
This document describes a flexural, non-resonance method for determining the components of the flexural complex modulus Ef* of polymers at frequencies typically in the range 0,01 Hz to 100 Hz. Higher-frequency measurements can be made, but significant errors in the dynamic properties measured are likely to result (see 10.2.2 and 10.2.3). The method is suitable for measuring dynamic storage moduli in the range 10 MPa to 200 GPa.
Although materials with moduli less than 10 MPa can be studied, more accurate measurements of their dynamic-mechanical properties can be made using shear modes of deformation (see ISO 6721-6).
This method is particularly suited to the measurement of loss factors greater than 0,02 and can therefore be conveniently used to study the variation of dynamic properties with temperature and frequency through most of the glass-rubber relaxation region (see ISO 6721-1). The availability of data determined over wide ranges of both frequency and temperature enables master plots to be derived, using frequency/temperature shift procedures, which present dynamic properties over an extended frequency range at different temperatures.
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 2 | National foreword |
| 6 | Foreword |
| 7 | 1 Scope 2 Normative references 3 Terms and definitions 4 Principle |
| 8 | 5 Apparatus 5.1 Loading assembly 5.1.1 General 5.1.2 Load stage 5.1.3 Transducers |
| 9 | 5.2 Electronic data-processing equipment 5.3 Temperature measurement and control 5.4 Devices for measuring test specimen dimensions 6 Test specimens 6.1 General 6.2 Shape and dimensions 6.3 Preparation 7 Number of specimens 8 Conditioning |
| 10 | 9 Procedure 9.1 Test atmosphere 9.2 Measuring the cross-section of the specimen 9.3 Clamping the specimen 9.4 Varying the temperature 9.5 Performing the test |
| 11 | 10 Expression of results 10.1 Symbols 10.2 Calculation of flexural storage modulus Ef′ 10.2.1 General |
| 12 | 10.2.2 Avoidance of specimen resonance |
| 13 | 10.2.3 Correction for transducer resonance 10.2.4 Correction for apparatus compliance 10.2.5 Application of a length correction |
| 14 | 10.3 Calculation of the flexural loss factor tan  10.4 Calculation of the flexural loss modulus Ef′′ 10.5 Presentation of data as a function of temperature 11 Precision 12 Test report |
| 17 | Bibliography |
