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BS ISO 13084:2018

$142.49

Surface chemical analysis. Secondary ion mass spectrometry. Calibration of the mass scale for a time-of-flight secondary ion mass spectrometer

Published By Publication Date Number of Pages
BSI 2018 24
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This document specifies a method to optimize the mass calibration accuracy in time-of-flight secondary ion mass spectrometry (SIMS) instruments used for general analytical purposes. It is only applicable to time-of-flight instruments but is not restricted to any particular instrument design. Guidance is provided for some of the instrumental parameters that can be optimized using this procedure and the types of generic peaks suitable to calibrate the mass scale for optimum mass accuracy.

PDF Catalog

PDF Pages PDF Title
2 National foreword
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
4 Symbols and abbreviated terms
4.1 Symbols
10 4.2 Abbreviated terms
5 Outline of method
11 6 Method for improving mass accuracy
6.1 Obtaining the reference sample for optimization
12 6.2 Preparation of polycarbonate sample
6.3 Obtaining the SIMS spectral data
13 6.4 Calculating mass accuracy
15 6.5 Optimizing instrumental parameters
17 6.6 Calibration procedure
19 Annex A (informative) Calibration uncertainty
21 Annex B (informative) Internal addition method
23 Bibliography
BS ISO 13084:2018
$142.49