BS EN 12014-2:2017 – TC:2020 Edition

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Tracked Changes. Foodstuffs. Determination of nitrate and/or nitrite content – HPLC/IC method for the determination of nitrate content of vegetables and vegetable products

Published By	Publication Date	Number of Pages
BSI	2020	55

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Categories: 67.080.20 - Vegetables and derived products, BSI

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Description

This European Standard specifies a high-performance liquid chromatographic (HPLC) and an ion chromatographic (IC) method for determination of the nitrate level in vegetables and vegetable products. This method is applicable for samples with a content of 25 mg/kg or greater. It has been validated on naturally contaminated and spiked samples as beetroot juice with nitrate mass fractions of 194 mg/kg and 691 mg/kg, pureed carrots with nitrate mass fractions of 26 mg/kg and 222 mg/kg and with iceberg lettuce with nitrate mass fractions of 623 mg/kg and 3 542 mg/kg.

PDF Catalog

PDF Pages	PDF Title
35	undefined
40	1 Scope 2 Normative references 3 Principle 4 Reagents
41	5 Apparatus and equipment
42	6 Procedure 6.1 Sample preparation 6.1.1 Liquid samples, e.g. vegetable juice 6.1.2 Solid samples, e.g. leaf vegetable 6.1.3 Pasty samples, e.g. mashed vegetables 6.2 Hot water extraction of samples (solid and pasty samples) 6.3 Preparation of sample test solutions 6.4 Preparation of the calibration curve
43	6.5 Determination 6.5.1 High-performance liquid chromatography 6.5.2 Ion chromatography 7 Evaluation 7.1 Identification and quantitative determination 7.2 Calculation 7.3 Precision 7.3.1 General
44	7.3.2 Repeatability 7.3.3 Reproducibility 8 Test report
45	Annex A (informative)Examples of HPLC/IC chromatograms
48	Annex B (informative)Precision data
50	Annex C (informative)Examples of suitable HPLC conditions
51	Annex D (informative)Examples of suitable IC conditions

Additional information

Status	Confirmed
Pages	55
Publication Date	2020-02-26
ISBN	978 0 539 10078 5
Standard Number	BS EN 12014-2:2017 – TC
Title	Tracked Changes. Foodstuffs. Determination of nitrate and/or nitrite content – HPLC/IC method for the determination of nitrate content of vegetables and vegetable products
Descriptors	Food products, Vegetables, Chemical analysis and testing, Bibliography, Chromatography, Nitrites, Specimen preparation, Nitrates, Food testing, Reproducibility, Vegetable juices, Determination of content, Liquid chromatography
Publisher	BSI
Committee	AW/275
ICS Codes	67.080.20 - Vegetables and derived products

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BS EN 12014-2:2017 – TC:2020 Edition

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