{"id":318236,"date":"2024-10-19T21:58:31","date_gmt":"2024-10-19T21:58:31","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-iso-179472014\/"},"modified":"2024-10-25T20:15:56","modified_gmt":"2024-10-25T20:15:56","slug":"bs-iso-179472014","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-iso-179472014\/","title":{"rendered":"BS ISO 17947:2014"},"content":{"rendered":"

This International Standard specifies the methods for the chemical analysis of fine silicon nitride powders used as the raw material for fine ceramics.<\/p>\n

This International Standard stipulates the determination methods of total silicon, total nitrogen, aluminium, iron, calcium, oxygen, carbon, fluorine, and chlorine in fine silicon nitride powders.<\/p>\n

PDF Catalog<\/h4>\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n
PDF Pages<\/th>\nPDF Title<\/th>\n<\/tr>\n
7<\/td>\nForeword <\/td>\n<\/tr>\n
8<\/td>\nIntroduction <\/td>\n<\/tr>\n
9<\/td>\nSection sec_1
Section sec_2
1\tScope
2\tNormative references <\/td>\n<\/tr>\n
10<\/td>\nSection sec_3
Section sec_4
Section sec_4.1
Section sec_4.2
Section sec_4.3
Section sec_5
Section sec_6
3\tAnalytes and ranges
4\tPreparation of test sample
4.1\tSampling
4.2\tDrying
4.3\tWeighing
5\tApparatus and reagents
6\tBlank test <\/td>\n<\/tr>\n
11<\/td>\nSection sec_7
Section sec_7.1
Section sec_7.2
Section sec_7.2.1
Section sec_7.2.2
Section sec_7.2.2.1
Section sec_7.2.2.2
Section sec_7.2.2.3
Section sec_7.2.2.4
Section sec_7.2.2.5
Section sec_7.2.2.6
Section sec_7.2.2.7
Section sec_7.2.3
Section sec_7.2.3.1
Section sec_7.2.3.2
Section sec_7.2.3.3
Section sec_7.2.3.4
7\tDetermination of total silicon
7.1\tClassification of determination methods
7.2\tFusion\u2011dehydration\/insolubilization separation\u2011gravimetry and ICP-OES <\/td>\n<\/tr>\n
12<\/td>\nSection sec_7.2.3.5
Section sec_7.2.3.6
Section sec_7.2.4
Section sec_7.2.4.1
Section sec_7.2.4.2
Section sec_7.2.4.3
Section sec_7.2.4.4
Section sec_7.2.5
Section sec_7.2.6 <\/td>\n<\/tr>\n
13<\/td>\nSection sec_7.2.7
Section sec_7.3
Section sec_8
Section sec_8.1
Section sec_8.2
Section sec_8.2.1
Section sec_8.2.2
Section sec_8.2.2.1
Section sec_8.2.2.2
7.3\tXRF using fused cast-bead method
8\tDetermination of total nitrogen
8.1\tClassification of determination methods
8.2\tAcid pressure decomposition\u2011distillation separation\u2011acidimetric titration method <\/td>\n<\/tr>\n
14<\/td>\nSection sec_8.2.2.3
Section sec_8.2.2.4
Section sec_8.2.2.5
Section sec_8.2.2.6
Section sec_8.2.2.7
Section sec_8.2.2.8
Section sec_8.2.2.9
Section sec_8.2.2.10
Section sec_8.2.3
Section sec_8.2.3.1
Section sec_8.2.3.2 <\/td>\n<\/tr>\n
15<\/td>\nSection sec_8.2.3.3
Section sec_8.2.3.4
Table tab_d
Figure fig_1 <\/td>\n<\/tr>\n
16<\/td>\nTable tab_e
Figure fig_2
Section sec_8.2.3.5
Section sec_8.2.3.6
Section sec_8.2.3.7 <\/td>\n<\/tr>\n
17<\/td>\nSection sec_8.2.3.8
Section sec_8.2.3.9
Section sec_8.2.3.10
Section sec_8.2.3.11
Section sec_8.2.4
Section sec_8.2.5 <\/td>\n<\/tr>\n
18<\/td>\nSection sec_8.2.6
Section sec_8.3
Section sec_8.3.1
Section sec_8.3.2
Section sec_8.3.2.1
Section sec_8.3.2.2
Section sec_8.3.3
Section sec_8.3.3.1
Section sec_8.3.3.2
8.3\tInert gas fusion\u2011thermal conductivity method <\/td>\n<\/tr>\n
19<\/td>\nFigure fig_3
Section sec_8.3.4
Section sec_8.3.4.1
Section sec_8.3.4.2
Section sec_8.3.4.3
Section sec_8.3.4.4 <\/td>\n<\/tr>\n
20<\/td>\nTable tab_h
Figure fig_4
Section sec_8.3.5
Section sec_8.3.6
Section sec_8.3.7 <\/td>\n<\/tr>\n
21<\/td>\nSection sec_8.3.8
Section sec_8.4
Section sec_9
Section sec_9.1
Section sec_9.2
8.4\tFusion\u2011ammonia separation\u2011acidimetric titration method
9\tDetermination of aluminium, iron, and calcium
9.1\tPrinciple
9.2\tReagents <\/td>\n<\/tr>\n
22<\/td>\nSection sec_9.2.1
Section sec_9.2.2
Section sec_9.2.3
Section sec_9.2.4
Section sec_9.2.5
Section sec_9.2.6
Section sec_9.2.7
Section sec_9.2.8
Section sec_9.3
Section sec_9.3.1
Section sec_9.3.2
Section sec_9.3.3
Section sec_9.3.4
Section sec_9.3.5
Section sec_9.3.6
Section sec_9.3.7
Section sec_9.4
9.3\tApparatus and instrument
9.4\tProcedure <\/td>\n<\/tr>\n
23<\/td>\nSection sec_9.5
Section sec_9.6
Section sec_9.7
9.5\tBlank test
9.6\tDrawing calibration curve
9.7\tCalculation <\/td>\n<\/tr>\n
24<\/td>\nSection sec_10
Section sec_10.1
Section sec_10.2
Section sec_10.3
Section sec_10.4
Section sec_10.5
Section sec_10.6
Section sec_10.7
10\tDetermination of oxygen
10.1\tPrinciple
10.2\tReagents
10.3\tApparatus
10.4\tInstrument
10.5\tProcedure
10.6\tBlank test
10.7\tCalculation of calibration coefficient <\/td>\n<\/tr>\n
25<\/td>\nSection sec_10.8
Section sec_11
Section sec_11.1
Section sec_11.2
Section sec_11.2.1
10.8\tCalculation
11\tDetermination of carbon
11.1\tClassification of determination methods
11.2\tCombustion (RF furnace)\u2011IR absorption spectrometry <\/td>\n<\/tr>\n
26<\/td>\nSection sec_11.2.2
Section sec_11.2.2.1
Section sec_11.2.2.2
Section sec_11.2.3
Section sec_11.2.3.1
Section sec_11.2.3.2
Section sec_11.2.4
Table tab_o
Figure fig_5
Section sec_11.2.4.1
Section sec_11.2.4.2
Section sec_11.2.4.3
Section sec_11.2.4.4 <\/td>\n<\/tr>\n
27<\/td>\nSection sec_11.2.5
Section sec_11.2.6
Section sec_11.2.7 <\/td>\n<\/tr>\n
28<\/td>\nSection sec_11.2.8
Section sec_11.3
Section sec_11.4
Section sec_11.5
Section sec_12
Section sec_12.1
Section sec_12.2
Section sec_12.2.1
Section sec_12.2.2
Section sec_12.2.3
Section sec_12.2.4
Section sec_12.2.5
Section sec_12.2.6
11.3\tCombustion (resistance furnace)\u2011coulometry
11.4\tCombustion (resistance furnace)\u2011gravimetry
11.5\tCombustion (resistance furnace)\u2011conductometry
12\tDetermination of fluorine and chlorine
12.1\tPrinciple
12.2\tReagents <\/td>\n<\/tr>\n
29<\/td>\nSection sec_12.2.7
Section sec_12.2.8
Section sec_12.2.9
Section sec_12.2.10
Section sec_12.3
Section sec_12.3.1
Section sec_12.3.1.1
Section sec_12.3.1.2
Section sec_12.3.1.3
Section sec_12.3.1.4
Section sec_12.3.1.5
Section sec_12.3.1.6
Section sec_12.3.1.7
Section sec_12.3.2
Section sec_12.3.3
Section sec_12.4
Section sec_12.4.1
Section sec_12.4.2
12.3\tApparatus and instruments
12.4\tProcedure <\/td>\n<\/tr>\n
30<\/td>\nSection sec_12.4.2.1
Section sec_12.4.2.2
Section sec_12.4.2.3
Section sec_12.5
Section sec_12.6
Section sec_12.7
12.5\tBlank test
12.6\tDrawing calibration curve
12.7\tCalculation <\/td>\n<\/tr>\n
31<\/td>\nSection sec_13
Section sec_13.1
Section sec_13.2
Section sec_13.3
Table tab_1
13\tReporting analytical values
13.1\tNumber of analyses
13.2\tEvaluation of analytical values
13.3\tExpression of analytical values <\/td>\n<\/tr>\n
32<\/td>\nSection sec_14
14\tTest report <\/td>\n<\/tr>\n
33<\/td>\nAnnex sec_A
Annex\u00a0A
\n(informative)<\/p>\n

List of commercial certified reference materials <\/td>\n<\/tr>\n

34<\/td>\nAnnex sec_B
Table tab_B.1
Annex\u00a0B
\n(informative)<\/p>\n

Analytical results obtained from a round robin test <\/td>\n<\/tr>\n

35<\/td>\nTable tab_u
Table tab_B.2 <\/td>\n<\/tr>\n
36<\/td>\nTable tab_v
Table tab_B.3 <\/td>\n<\/tr>\n
37<\/td>\nTable tab_w
Table tab_B.4 <\/td>\n<\/tr>\n
38<\/td>\nTable tab_x <\/td>\n<\/tr>\n
39<\/td>\nAnnex sec_C
Annex\u00a0C
\n(informative)<\/p>\n

Spectral lines for ICP-OES <\/td>\n<\/tr>\n

40<\/td>\nReference ref_1
Reference ref_2
Reference ref_3
Reference ref_4
Reference ref_5
Reference ref_6
Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"

Fine ceramics (advanced ceramics, advanced technical ceramics). Methods for chemical analysis of fine silicon nitride powders<\/b><\/p>\n\n\n\n\n
Published By<\/td>\nPublication Date<\/td>\nNumber of Pages<\/td>\n<\/tr>\n
BSI<\/b><\/a><\/td>\n2014<\/td>\n44<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":318240,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[1164,2641],"product_tag":[],"class_list":{"0":"post-318236","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-81-060-30","7":"product_cat-bsi","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/318236","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/318240"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=318236"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=318236"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=318236"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}