{"id":309179,"date":"2024-10-19T21:13:47","date_gmt":"2024-10-19T21:13:47","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-iso-46522020\/"},"modified":"2024-10-25T18:55:13","modified_gmt":"2024-10-25T18:55:13","slug":"bs-iso-46522020","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-iso-46522020\/","title":{"rendered":"BS ISO 4652:2020"},"content":{"rendered":"
This document specifies two methods for the determination of the specific surface area of types and grades of carbon black for use in the rubber industry:<\/p>\n
method A: automatic gas chromatography method (carrier gas method);<\/p>\n<\/li>\n
method B: automatic volumetric method.<\/p>\n<\/li>\n<\/ol>\n
Somewhat different results might be obtained from the two methods. The degassing procedure differs between method A and method B, and it is important to investigate the possibility of correcting the results by using standard reference blacks.<\/p>\n
The results might also differ from those obtained using the multipoint method specified in ISO 18852<\/span><\/span>, which is the preferred method.<\/p>\n These methods are not applicable to porous carbon blacks.<\/p>\n Rubber compounding ingredients. Carbon black. Determination of specific surface area by nitrogen adsorption methods. Single-point procedures<\/b><\/p>\nPDF Catalog<\/h4>\n
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\n PDF Pages<\/th>\n PDF Title<\/th>\n<\/tr>\n \n 2<\/td>\n National foreword <\/td>\n<\/tr>\n \n 6<\/td>\n Foreword <\/td>\n<\/tr>\n \n 7<\/td>\n Introduction <\/td>\n<\/tr>\n \n 9<\/td>\n 1 Scope
2 Normative references
3 Terms and definitions
4 Method A: Automatic gas chromatography (carrier gas method)
4.1 Principle <\/td>\n<\/tr>\n\n 10<\/td>\n 4.2 Apparatus <\/td>\n<\/tr>\n \n 11<\/td>\n 4.3 Reagents
4.4 Preparation of the sample portion
4.5 Degassing of sample <\/td>\n<\/tr>\n\n 12<\/td>\n 4.6 Measurement procedure
4.7 Validation <\/td>\n<\/tr>\n\n 13<\/td>\n 4.8 Expression of results
4.8.1 Results without correction
4.8.2 Results with correction
4.9 Correction by the multipoint nitrogen surface area (optional) <\/td>\n<\/tr>\n\n 14<\/td>\n 4.10 Test report
5 Method B: Automatic volumetric method
5.1 Principle
5.2 Apparatus <\/td>\n<\/tr>\n\n 16<\/td>\n 5.3 Reagents
5.4 Preparation of automatic volumetric adsorption measurement apparatus <\/td>\n<\/tr>\n\n 17<\/td>\n 5.5 Degassing of sample
5.5.1 General
5.5.2 Vacuum suction method
5.5.3 Purge gas flow method <\/td>\n<\/tr>\n\n 18<\/td>\n 5.6 Measurement procedure
5.7 Validation with SRB
5.8 Expression of results
5.9 Correction by the multipoint nitrogen surface area (optional)
5.10 Test report <\/td>\n<\/tr>\n\n 19<\/td>\n 6 Precision <\/td>\n<\/tr>\n \n 20<\/td>\n Annex A (informative) Correction by the multipoint nitrogen surface area <\/td>\n<\/tr>\n \n 21<\/td>\n Annex B (informative) Precision <\/td>\n<\/tr>\n \n 23<\/td>\n Bibliography <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":" \n\n
\n Published By<\/td>\n Publication Date<\/td>\n Number of Pages<\/td>\n<\/tr>\n \n BSI<\/b><\/a><\/td>\n 2020<\/td>\n 24<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":309187,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[1173,2641],"product_tag":[],"class_list":{"0":"post-309179","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-83-040-20","7":"product_cat-bsi","9":"first","10":"instock","11":"sold-individually","12":"shipping-taxable","13":"purchasable","14":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/309179","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/309187"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=309179"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=309179"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=309179"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}