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BS EN 14242:2023

BS EN 14242:2023

$142.49

Aluminium and aluminium alloys. Chemical analysis. Inductively coupled plasma optical emission spectrometric analysis

Published By Publication Date Number of Pages
BSI 2023 24
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This document specifies an inductively coupled plasma optical emission spectrometric method (ICP-OES) for the analysis of aluminium and aluminium alloys. This method is applicable to the determination of silicon, iron, copper, manganese, magnesium, chromium, nickel, zinc, titanium, gallium, vanadium, beryllium, bismuth, calcium, cadmium, cobalt, lithium, sodium, lead, antimony, tin, strontium and zirconium in aluminium and aluminium alloys. The content of the elements to be determined should be at least 10 times higher than the corresponding detection limits.

PDF Catalog

PDF Pages PDF Title
2 undefined
6 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
7 5 Reagents
12 6 Apparatus
13 7 Sampling
7.1 General
7.2 Test sample
8 Procedure
8.1 Test portion
8.2 Dissolution procedure I with sodium hydroxide solution
14 8.3 Dissolution procedure II with nitric acid and hydrofluoric acid
8.4 Dissolution procedure III with a mixture of hydrochloric acid and nitric acid
15 8.5 Dissolution procedure IV with hydrochloric acid
8.6 Calibration solutions and drift correction solution
8.6.1 General
16 8.6.2 Preparation of the calibration solutions
8.7 Measurements
8.7.1 Adjustment of the apparatus
8.7.2 Measurement of the calibration solutions
17 8.7.3 Measurement of the test solutions
8.8 Calibration curves
9 Correction of short-term fluctuations and drift
9.1 General
9.2 Short-term fluctuations
9.3 Drift
10 Investigation of interferences
18 11 Expression of the results
11.1 Correction
11.2 Result
12 Test report
19 Annex A (informative)Analytical wavelengths
21 Annex B (informative)Plasma optical emission spectrometer — Suggested performance criteria to be checked
B.1 Short- and long-term stability
B.2 Evaluating the background equivalent concentration
22 B.3 Evaluating the limit of detection
B.4 Linearity of the calibration curves

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BS EN 14242:2023
$142.49