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BS EN ISO 16181-2:2021

BS EN ISO 16181-2:2021

$142.49

Footwear. Critical substances potentially present in footwear and footwear components – Determination of phthalate without solvent extraction

Published By Publication Date Number of Pages
BSI 2021 30
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This document specifies a method for the determination of the content of specific phthalates (see Annex A) by pyrolyzer/thermal desorption gas chromatography-mass spectrometry (Py/TD-GC-MS). This document is applicable to all types of footwear materials except textiles.

NOTE

See also CEN/TR 16417 for a list of the specific phthalates to which this document applies.

PDF Catalog

PDF Pages PDF Title
2 National foreword
4 European foreword
6 Foreword
7 1 Scope
2 Normative references
3 Terms and definitions
4 Principle
8 5 Apparatus
6 Reagents and materials
9 7 Sampling
8 Test procedure
8.1 Test sample preparation
8.2 Calibration
10 8.3 Chromatographic analysis
8.3.1 The chromatography parameters for gas chromatograph – mass spectrometer equipped with a pyrolyzer
8.3.2 Qualitative and quantitative analysis by gas chromatograph – mass spectrometer equipped with a pyrolyzer
9 Calculation of phthalate compounds in the sample
9.1 Calculation of the phthalate compounds in the sample
11 9.2 Performance of the test method
10 Detection limit
11 Test report
12 Annex A (informative) List of phthalates specified in CEN/TR 16417
15 Annex B (informative) Sampling guidelines
18 Annex C (informative) Chromatography parameters for gas chromatography mass spectrometry equipped with a pyrolyzer
20 Annex D (informative) Verification of the evolved gas analysis (EGA) thermal desorption zone
22 Annex E (informative) Examples of chromatogram for phthalate by Py/TD-GC-MS
24 Annex F (informative) Comparative test results of ISO 16181-1 and this document (i.e. ISO 16181-2)
28 Bibliography

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BS EN ISO 16181-2:2021
$142.49