BSI PD IEC TS 62607-4-7:2018
$142.49
Nanomanufacturing. Key control characteristics – Nano-enabled electrical energy storage. Determination of magnetic impurities in anode nanomaterials, ICP-OES method
| Published By | Publication Date | Number of Pages |
| BSI | 2018 | 24 |
This part of IEC TS 62607 provides a method for the determination of magnetic impurities in anode nanomaterials for energy storage devices using an Inductively Coupled Plasma Optical Emission Spectrometer (ICP-OES), including test overview, reagents, apparatus, test procedures, test results and test report.
This document applies to the determination of the total content of magnetic impurities (iron, cobalt, chromium, and nickel) ≥ 0,02 mg/kg which can be attracted by magnet.
PDF Catalog
| PDF Pages | PDF Title |
|---|---|
| 2 | undefined |
| 4 | CONTENTS |
| 6 | FOREWORD |
| 8 | INTRODUCTION |
| 9 | 1 Scope 2 Normative references 3 Terms and definitions |
| 10 | 4 Overview of the measurement 5 Reagents 5.1 Nitric acid 5.2 Hydrochloric acid 5.3 Nitrohydrochloric acid 5.4 Ethanol 5.5 Argon gas 5.6 Standard solutions 5.6.1 Iron standard solution 5.6.2 Cobalt standard solution, 5.6.3 Chromium standard solution, 5.6.4 Nickel standard solution, 6 Apparatus 6.1 ICP-OES |
| 11 | 6.2 Conical flask 6.3 Sample tank 6.4 Magnet 6.5 Electronic balance 6.6 Scroll equipment 6.7 Ultrasonic cleaning equipment 6.8 Heating device 7 Preparation of series of standard solutions Tables Table 1 –Recommended test wavelengths for the determination of magnetic impurities |
| 12 | 8 Test procedure 8.1 Cleaning the magnet 8.2 Test sample 8.3 Attraction of magnetic impurities 8.4 Remove nonmagnetic impurities Table 2 – Correspondence of the measured mass to the untapped bulk density of the sample |
| 13 | 8.5 Extraction of magnetic impurities 8.6 Preparation of blank sample 8.7 Test 9 Data analysis and calculation of results Table 3 – Instrument operating parameters |
| 14 | 10 Test report |
| 15 | Annex A (informative)Diagram of the scroll device Figures Figure A.1 – Diagram of sample tank on the rolling device |
| 16 | Annex B (informative)Magnet removal method Figure B.1 – Diagram of magnet removal |
| 17 | Annex C (informative)Case study C.1 Preparation of series of standard solutions C.2 Cleaning the magnet C.3 Weighing sample Figure C.1 – Procedure for cleaning the magnet |
| 18 | C.4 Attraction of magnetic impurities C.5 Remove nonmagnetic impurities Figure C.2 – Procedure for weighing sample Figure C.3 – Procedure for attraction of magnetic impurities |
| 19 | C.6 Extraction of magnetic impurities C.7 Test Figure C.4 – Procedure for removing nonmagnetic impurities Figure C.5 – Procedure for extraction of magnetic impurities |
| 20 | C.8 Identify the uncertainty sources Table C.1 – Test results of magnetic impurities |
| 21 | Annex D (informative)Validation of the attraction procedure D.1 Experimental samples D.2 Experimental procedure D.3 Experimental results and conclusion Table D.1 – Test results of magnetic impurities |
| 22 | Bibliography |
