ASTM-D3612:2002 Edition
$58.50
D3612-02e1 Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
Published By | Publication Date | Number of Pages |
ASTM | 2002 | 22 |
ASTM D3612-02e1
Historical Standard: Standard Test Method for Analysis of Gases Dissolved in Electrical Insulating Oil by Gas Chromatography
ASTM D3612
Scope
1.1 This test method covers three procedures for extraction and measurement of gases dissolved in electrical insulating oil having a viscosity of 20 cSt (100 SUS) or less at 40°C (104°F), and the identification and determination of the individual component gases extracted. Other methods have been used to perform this analysis.
1.2 The individual component gases that may be identified and determined include:
1.3 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney, and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements see 6.1.8, 30.2.2 and 30.3.1.
Keywords
capillary columns; combustible gases; dissolved gases; gases; headspace; insulating oil; oil; transformer oil; Dissolved gases; Electrical insulating oils; Gas chromatography (GC)–insulating materials/applications; Gas content
ICS Code
ICS Number Code 29.040.10 (Insulating oils)
DOI: 10.1520/D3612-02E01
PDF Catalog
PDF Pages | PDF Title |
---|---|
1 | Scope Referenced Documents Terminology |
2 | Summary of Test Method Significance and Use Apparatus Sampling |
3 | FIG. 1 FIG. 2 |
4 | Method A—Vacuum Extraction Preparation of Apparatus Procedure FIG. 3 |
5 | Apparatus Reagent and Materials |
6 | Calibration FIG. 4 |
7 | Procedure Calculation Report Precision and Bias TABLE 1 |
8 | Method B—Stripper Column Extraction Apparatus Reagent and Materials |
9 | FIG. 5 |
10 | Calibration (Gases) Efficiency Determination Procedure for Direct Injection Calculation Report Precision and Bias |
11 | TABLE 2 TABLE 3 |
12 | FIG. 6 |
13 | Method C—Headspace sampling Apparatus |
14 | Chemicals Procedure FIG. 7 TABLE 4 TABLE 5 |
15 | FIG. 8 |
16 | Determination of Partition Coefficients TABLE 6 |
17 | Calculation Report Precision and Bias Keywords |
18 | A1. PREPARATION OF SMALL QUANTITIES OF GAS-IN-OIL STANDARDS (Mandatory Information—Method B) A1.1 Calibration Apparatus A1.2 Procedure TABLE 7 |
19 | A2. PREPARATION OF LARGE QUANTITIES OF GAS-IN-OIL STANDARDS (Mandatory Information—Method B) A2.1 Apparatus A2.2 Materials A2.3 Preparation of Apparatus FIG. A2.1 FIG. A2.2 |
20 | A2.4 Procedure A2.5 Calculation A2.6 Reliability FIG. A2.3 |
21 | X1. PRECISION AND BIAS OF GAS RATIOS USED IN FAULT DIAGNOSIS IN OIL-INSULATED ELECTRICAL EQUIPMENT X1.1 FIG. X1.1 |